By Hans Zimmer
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Additional resources for Annual Reports in Inorganic and General Syntheses–1975
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It was also shown that tBu2SiHCl and not tBu2Cl2 couples with the third mole ^BuLi (34,35). Since replacement reactions are faster for the silylfluoride than the silyl chloride, reaction of a RoSiHF spe cies seems to be the key to addition of a 3rd bulky group. Silicon tetra chloride and ^BuLi heated in the absence of solvent also gave ^Bu3SiH (36). When the steric bulk is reduced from "^Bu to iPr it is possible to generate ipr4Si (in small yields) and again the key step is reaction of iPr3SiF with iPrLi (37).
Annual Reports in Inorganic and General Syntheses–1975 by Hans Zimmer