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By Hans Zimmer

ISBN-10: 0120407043

ISBN-13: 9780120407040

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P. B u k o v e c and J. S i f t e r , M O N A T S H . S. B a t s a n o v , ZH. N E O R G . , 2i0, 826 ( 1 9 7 5 ) . N . W . A l c o c k and H . D . B . J e n k i n s , J. CHEM. S O C , D A L T O N T R A N S . , 1907 ( 1 9 7 4 ) . J. G. T u c k , J. CHEM. S O C , CHEM. , 600 ( 1 9 7 5 ) . G. Joy, A . P . G a n g h a n , I. F. P. D o u g h e r t y , INORG. , Γ 4 , 1795 ( 1 9 7 5 ) . G. T h i e l e and W. R i n k , Z. A N O R G . A L L G . , 4 1 £ , 231 (1975). G. T h i e l e and W. R i n k , Z. A N O R G .

S. Kohama, S. Matsumoto, KAGUKU TO KOGYO, 48, 308 (1974). 129. G. M. A. Samsonova, Yu. A. M. Kudyakov, IZV. AKAD. NAUK SSSR, SER. , 2794 (1974). 130. G. S. M. P. N. Vlasova, ZH. OBSHCH. , 45, 1649 (1975). 131. M. G. S. M. D'yakov, ZH. OBSHCH. , 45, 1394 (1975). 132. G. S. P. M. N. N. Tandura, ZH. OBSHCH. , 45, 1395 (1975). 133. G. M. I. Gubanova, ZH. OBSHCH. , 45, 1905 (1975). 134. G. M. P. N. F. Miro­ nov, ZH. OBSHCH. KHIM. , 45, 1902 (1975). 135. G. M. S. N. F. Cher­ nov, ZH. OBSHCH. , 45, 1901 (1975).

It was also shown that tBu2SiHCl and not tBu2Cl2 couples with the third mole ^BuLi (34,35). Since replacement reactions are faster for the silylfluoride than the silyl chloride, reaction of a RoSiHF spe­ cies seems to be the key to addition of a 3rd bulky group. Silicon tetra­ chloride and ^BuLi heated in the absence of solvent also gave ^Bu3SiH (36). When the steric bulk is reduced from "^Bu to iPr it is possible to generate ipr4Si (in small yields) and again the key step is reaction of iPr3SiF with iPrLi (37).

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Annual Reports in Inorganic and General Syntheses–1975 by Hans Zimmer


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